Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C30H44O5 |
| M r | 484.65 |
| Crystal system, space group | Monoclinic, P21 |
| Temperature (K) | 100 |
| a, b, c (Å) | 8.3465 (2), 10.9783 (3), 14.6583 (4) |
| β (°) | 101.056 (1) |
| V (Å3) | 1318.22 (6) |
| Z | 2 |
| Radiation type | Cu Kα |
| μ (mm−1) | 0.64 |
| Crystal size (mm) | 0.45 × 0.23 × 0.12 |
| Data collection | |
| Diffractometer | Bruker SMART APEX CCD area-detector |
| Absorption correction | Multi-scan (SADABS; Bruker, 2009 ▸) |
| T min, T max | 0.760, 0.927 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 28696, 5116, 5023 |
| R int | 0.042 |
| (sin θ/λ)max (Å−1) | 0.618 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.041, 0.115, 1.06 |
| No. of reflections | 5116 |
| No. of parameters | 325 |
| No. of restraints | 2 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.70, −0.31 |
| Absolute structure | Flack, 1983 ▸ |
| Absolute structure parameter | 0.14 (17) |