Skip to main content
. 2017 Apr 13;7(1):109–114. doi: 10.15171/apb.2017.014

Table 1. NMR spectroscopic data of compound 1 .

Position δ C δ H ( J ) Position δ C δ H ( J )
2 165.47 - 1" 100.79 5.07,(d,8.4)
3 106.82 6.59, s 2" 83.22 *
4 183.37 - 3" 74.69 *
5 152.93 - 4" 70.46 *
6 116.02 - 5" 76.45 *
7 172.08 - 6" 64.03 *
8 102.80 6.70, s 1'" 103.55 4.54
8a 150.78 - 2'" 72.03 *
4a 101.57 - 3'" 67.33 *
9 prenyl 22.76 overlapped 4'" 71.55 *
10 122.90 5.36, br t 5'" 72.41 *
11 128.68 - 6'" 63.77 *
12 19.95 1.34, s - - -
13 25.01 1.29, s - - -
1' 122.13 - - - -
2' 128.86 7.89,(d,8.4) - - -
3' 116.02 6.94,(d,8.4) - - -
4' 161.87 - - - -
5' 116.02 6.94,(d,8.4) - - -
6' 128.86 7.89,(d,8.4) - - -
OCO-CH3 20.01 2.19, s - - -
OCO-CH3 176.82 - - - -

1H (200MHz) and 13C (50MHz) in CD3OD, δ in ppm, J in Hz) ; * overlapping signals in 3.5-4.5ppm.