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. 2015 Oct 21;79(3):455–462. doi: 10.1021/acs.jnatprod.5b00604

Table 1. 1H (600 MHz) and 13C (100 MHz) NMR Data for Compounds 1 and 2 in DMSO-d6.

  1
2
no. δC δH, mult. (J in Hz) δC δH, mult. (J in Hz)
1 159.8, C   159.9, C  
2 89.0, CH 6.73, s 88.3, CH 6.79, s
3 155.3, C   155.5, C  
4 57.7, CH 4.55, qd (6.7, 6.6) 54.3, CH 4.65, qd (6.9, 6.6)
5 64.1, CH 4.43, ddd (8.8, 8.0, 6.7) 24.7, CH2 2.21, m; 1.71, m
6 39.3, CH2 2.67, dd (16.9, 8.0); 31.4, CH2 2.84, m; 2.45, m
    2.63, dd (16.9, 8.8)    
7 173.4, C   176.0, C  
8 13.3, CH3 1.23, d (6.5) 20.0, CH3 1.31, d (6.4)
1′ 163.7, C   163.7, C  
2′ 116.2, CH 5.98, m 116.2, CH 5.98, m
3′ 158.7, C   158.7, C  
4′ 28.0, CH3 2.03, d (1.2) 28.1, CH3 2.03, s
5′ 21.0, CH3 2.25, d (1.2) 21.1, CH3 2.25, s