|
Data collection statistics
|
| Wavelength (Å) |
0.9686 |
| Space group |
P212121
|
| Unit cell parameters: a, b, c (Å); α, β, γ (°) |
78.37, 86.63, 168.34; 90, 90, 90 |
| Resolution range (outer shell in brackets; Å) |
19.95–2.30 (2.37–2.30) |
| Unique reflections |
51 644 (4396) |
| Total observations |
319 802 (27 953) |
| <I / σ(I)>: all (outer shell) |
7.5 (1.9) |
| Rp.i.m.: all (outer shell) |
0.106 (0.979) |
| Completeness: all (outer shell) (%) |
99.9 (100) |
| Multiplicity |
6.1 (5.4) |
| Wilson B-factor |
33.9 |
|
Refinement statistics
|
| Protein non-hydrogen atoms |
8011 |
| Waters |
546 |
| Bond length deviation from ideal values (Å) |
0.0033 |
| Bond angle deviation from ideal values (°) |
0.53 |
| Ramachandran favoured/outliers (%) |
98.24/0 |
| All-atom clashscore |
1.37 |
| Rwork/Rfree (%) |
17.8/21.7 |
| MolProbity (32) score (percentile) |
0.87 (100) |
