Fig. 1. Molecular structure of 2. Solvent molecules and hydrogen atoms are omitted, and peripheral carbon atoms are depicted as wireframe, for clarity. Thermal ellipsoids drawn at 50% probability. Selected distances (Å) and angles (°): U1–Rh1: 2.7601(5), U1–I2: 2.9559(5), U1–I3: 3.0239(5), U1–O1: 2.123(2), U1–O2: 2.131(2), Rh1–I1: 2.6902(6), Rh1–P1: 2.2830(9), Rh1–P2: 2.2936(8), O1–U1–O2: 164.01(8), I2–U1–I3: 92.87(1), P1–Rh1–P2: 99.86(3), I1–Rh1–I1′: 78.62(1).
