Fig. 2. Molecular structure of 3. Solvent molecules and hydrogen atoms are omitted and peripheral carbon atoms are depicted as wireframe for clarity. Thermal ellipsoids drawn at 50% probability. Selected distances (Å) and angles (°): U1–Rh1: 2.7630(5), U1–I1: 3.0428(5), U1–I2: 3.2264(5), U–O: 2.129(4)–2.156(3), Rh1–I2: 2.7296(6), Rh–P: 2.318(1)–2.416(1), I1–U1–Rh1: 167.75(2), U1–I2–Rh1: 54.51(1).
