Table 1. Data collection and reduction statistics.
| λ, Å | 0.919 | 1.377 |
| Spacegroup | P4(3)32 | P4(3)32 |
| Cell dimensions | a = 62.16 Å | a = 62.21 Å |
| Resolution, Å | 27.8–1.44 | 31.1–1.65 |
| Total reflections | 173,047 (25,070)* | 170,252 (22,414) |
| Unique reflections | 7,922 (1117) | 5,475 (764) |
| Overall completeness, % | 100 (100) | 100 (100) |
| Anomalous completeness, % | — | 98.6 (99.7) |
| Rsym, % | 7.0 (35.8) | 8.1 (33.7) |
| Ranom, % | — | 9.5 (13.6) |
| Multiplicity | 21.8 (22.4) | 31.1 (29.3) |
| I/σ(I) | 9.3 (2.1) | 8.4 (2.1) |
| B factor from Wilson plot, Å2 | 9.15 | 7.21 |
| Phases FOM before solvent flattening | — | 0.25 |
| Phases FOM after solvent flattening | — | 0.78 |
FOM, figure of merit.
*
Numbers in parentheses refer to the high-resolution shell (1.52–1.44 for the 0.919-Å dataset and 1.73–1.65 for the 1.377-Å dataset)