Table 1.
Order | Total solid contents of concentrated decoction (%) | Mass ratio of ethanol to concentrated decoction (g/g) | Ethanol concentration (%) | Ethanol adding time (min) | Stirring speed (r/min) | Refrigeration temperature (°C) | Refrigeration time (h) |
DOE 1 | 50 | 3 | 89 | 30 | 400 | 25 | 12 |
DOE 2 | 30 | 3 | 95 | 10 | 400 | 25 | 36 |
DOE 3 | 50 | 1 | 95 | 30 | 200 | 25 | 36 |
DOE 4 | 30 | 3 | 89 | 30 | 400 | 5 | 36 |
DOE 5 | 30 | 1 | 95 | 10 | 400 | 25 | 12 |
DOE 6 | 30 | 1 | 89 | 30 | 200 | 25 | 36 |
DOE 7 | 50 | 1 | 89 | 10 | 400 | 5 | 36 |
DOE 8 | 50 | 3 | 89 | 10 | 200 | 25 | 12 |
DOE 9 | 50 | 3 | 95 | 10 | 200 | 5 | 36 |
DOE 10 | 30 | 3 | 95 | 30 | 200 | 5 | 12 |
DOE 11 | 50 | 1 | 95 | 30 | 400 | 5 | 12 |
DOE 12 | 30 | 1 | 89 | 10 | 200 | 5 | 12 |
DOE 13 | 40 | 2 | 92 | 20 | 300 | 15 | 24 |
DOE 14 | 40 | 2 | 92 | 20 | 300 | 15 | 24 |
DOE 15 | 40 | 2 | 92 | 20 | 300 | 15 | 24 |