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Synthesis of “Large” particles investigated as a function of heating rate. (A) Kinetics and temperature dependence of the Porod constant and Invariant. (B) Growth kinetics for radius and polydispersity of “Large” nanoparticles after nucleation. (C) Transmission electron micrographs of the particles after synthesis and the respective size distributions from image analysis for 1 K/min, 3 K/min, and 9 K/min heating rates.
