Table 1. Molar Ratios for NPs of Different Sizea.
NP size | Fe(CO)5/OA (molar ratio) | heating rates [K/min] |
---|---|---|
Small (3–4 nm) | 1:1.7 | 3, 9 |
Medium (5–6 nm) | 1:1.9 | 3 |
Large (9–10 nm) | 1:3.0 | 1, 3, 9 |
Experimental details for the NP synthesis experiments where the size was varied by Fe(CO)5/OA ratio and uniformity by heating rate.