Table 4.

Apparent recovery, signal suppression/enhancement, extraction recovery, and relative standard deviation of repeatability of R_A obtained for all of the selected mycotoxins and for each validated matrix, together with the validated LoQs.

Matrix		AFB1	OTA	FB1	DON	T-2	HT-2	ZEA
Bread	LoQ (μg/kg)	0.13	0.8	16	20	8	20	3.2
	RA (%)	61	64	84	62	65	62	65
	SSE (%)	83	98	113	61	55	63	75
	RE (%)	73	65	74	100	119	99	87
	RSDr (%)	14	10	15	18	17	15	20
Pasta	LoQ (μg/kg)	0.06	0.4	8	20	4	20	1.6
	RA (%)	61	79	116	69	75	79	75
	SSE (%)	52	102	120	66	96	109	83
	RE (%)	117	78	96	105	81	73	90
	RSDr (%)	11	12	11	12	16	15	16
Rice	LoQ (μg/kg)	0.06	0.4	8	20	4	20	1.6
	RA (%)	88	79	93	70	65	63	78
	SSE (%)	105	102	101	107	74	64	75
	RE (%)	83	78	92	65	88	98	104
	RSDr (%)	11	10	10	15	14	13	15
Wheat	LoQ (μg/kg)	0.06	0.4	8	20	4	20	1.6
	RA (%)	69	76	122	66	61	66	65
	SSE (%)	73	92	123	71	64	73	65
	RE (%)	94	83	99	92	95	90	101
	RSDr (%)	12	10	12	15	15	15	15
Backery products	LoQ (μg/kg)	0.13	0.8	16	20	8	20	3.2
	RA (%)	66	85	76	67	65	63	64
	SSE (%)	84	108	123	61	64	55	74
	RE (%)	79	79	61	109	102	116	87
	RSDr (%)	13	10	16	18	15	15	18
Breakfast cereals	LoQ (μg/kg)	0.13	0.8	16	20	8	20	3.2
	RA (%)	65	68	63	66	69	69	68
	SSE (%)	59	95	123	74	72	68	71
	RE (%)	110	71	52	89	96	101	96
	RSDr (%)	16	6	15	14	19	11	20