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. 2016 Jan 15;4(1):3. doi: 10.3390/diseases4010003

Table 1.

1H and 13C-NMR data for 8,8′-oxo-biplumbagin (1).

Position δH (I, m, J in Hz) δC HMBC (2J, 3J)
1,1′ - 185.2 -
2,2′ - 150.0 -
3,3′ 6.80, (2H, q, 1.6) 134.9 C1, C1′, C10, C10′, C11, C11′
4,4′ - 190.5 -
5,5′ - 161.3 -
6,6′ 7.29, (2H, d, 8.6) 124.3 C10, C10′, C5, C5′, C7, C7′, C8, C8′
7,7′ 7.20 (2H, d, 8.6) 137.9 C5, C5′, C6, C6′, C8, C8′, C9,C9′
8,8′ - 135.6 -
9, 9′ - 128.2 -
10, 10′ - 115.5 -
11,11′ 2.01 (6H, d, 1.6) C1, C1′, C2, C2′, C3, C3′
5-OH, 5′-OH 12.58 (2H, brs) - C10, C10′, C5, C5′, C6, C6′