Table 1.
Position | δH (I, m, J in Hz) | δC | HMBC (2J, 3J) |
---|---|---|---|
1,1′ | - | 185.2 | - |
2,2′ | - | 150.0 | - |
3,3′ | 6.80, (2H, q, 1.6) | 134.9 | C1, C1′, C10, C10′, C11, C11′ |
4,4′ | - | 190.5 | - |
5,5′ | - | 161.3 | - |
6,6′ | 7.29, (2H, d, 8.6) | 124.3 | C10, C10′, C5, C5′, C7, C7′, C8, C8′ |
7,7′ | 7.20 (2H, d, 8.6) | 137.9 | C5, C5′, C6, C6′, C8, C8′, C9,C9′ |
8,8′ | - | 135.6 | - |
9, 9′ | - | 128.2 | - |
10, 10′ | - | 115.5 | - |
11,11′ | 2.01 (6H, d, 1.6) | C1, C1′, C2, C2′, C3, C3′ | |
5-OH, 5′-OH | 12.58 (2H, brs) | - | C10, C10′, C5, C5′, C6, C6′ |