Stoe IPDS 1 diffractometer | 1721 independent reflections |
Radiation source: fine-focus sealed tube | 1038 reflections with I > 2σ(I) |
Plane graphite monochromator | Rint = 0.096 |
φ rotation scans | θmax = 25.3°, θmin = 2.7° |
Absorption correction: multi-scan (MULABS; Spek, 2009) | h = −17→17 |
Tmin = 0.985, Tmax = 1.000 | k = −20→20 |
13548 measured reflections | l = −35→35 |