Table 2. Experimental details.
| Crystal data | |
| Chemical formula | [AgCl(C7H7N3O2S)(C18H15P)2] |
| M r | 865.07 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 100 |
| a, b, c (Å) | 11.8581 (2), 28.5087 (4), 12.0272 (2) |
| β (°) | 104.9338 (17) |
| V (Å3) | 3928.57 (11) |
| Z | 4 |
| Radiation type | Cu Kα |
| μ (mm−1) | 6.33 |
| Crystal size (mm) | 0.25 × 0.23 × 0.18 |
| Data collection | |
| Diffractometer | Rigaku RAPID II curved image plate diffractometer |
| Absorption correction | Multi-scan (SCALEPACK; Otwinowski & Minor, 1997 ▸) |
| T min, T max | 0.253, 0.395 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 73254, 7590, 7495 |
| R int | 0.051 |
| (sin θ/λ)max (Å−1) | 0.618 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.027, 0.068, 1.08 |
| No. of reflections | 7590 |
| No. of parameters | 485 |
| No. of restraints | 2 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.43, −0.37 |