| Crystal data |
| Chemical formula |
C15H15NO2
|
|
M
r
|
241.28 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
293 |
|
a, b, c (Å) |
9.4257 (4), 12.2054 (5), 13.2067 (6) |
| α, β, γ (°) |
62.979 (3), 82.329 (3), 87.145 (3) |
|
V (Å3) |
1341.29 (10) |
|
Z
|
4 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.08 |
| Crystal size (mm) |
0.20 × 0.18 × 0.17 |
| |
| Data collection |
| Diffractometer |
Bruker SMART APEXII CCD |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2008 ▸) |
|
T
min, T
max
|
0.984, 0.987 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
31199, 4723, 3376 |
|
R
int
|
0.031 |
| (sin θ/λ)max (Å−1) |
0.595 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.046, 0.143, 1.09 |
| No. of reflections |
4723 |
| No. of parameters |
325 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.25, −0.20 |
