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. 2017 May 16;73(Pt 6):853–855. doi: 10.1107/S2056989017006995

Table 2. Experimental details.

Crystal data
Chemical formula Pb2(CrO4)(TeO3)
M r 705.98
Crystal system, space group Monoclinic, P21/n
Temperature (K) 296
a, b, c (Å) 7.4736 (12), 10.8091 (16), 9.4065 (14)
β (°) 111.098 (12)
V3) 708.95 (19)
Z 4
Radiation type Mo Kα
μ (mm−1) 52.91
Crystal size (mm) 0.09 × 0.06 × 0.01
 
Data collection
Diffractometer Bruker APEXII CCD
Absorption correction Multi-scan (SADABS; Bruker, 2015)
T min, T max 0.264, 0.494
No. of measured, independent and observed [I > 2σ(I)] reflections 23485, 2183, 1760
R int 0.094
(sin θ/λ)max−1) 0.717
 
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S 0.031, 0.070, 1.06
No. of reflections 2183
No. of parameters 100
Δρmax, Δρmin (e Å−3) 2.47, −2.33

Computer programs: APEX3 and SAINT (Bruker, 2015), SHELXL2014 (Sheldrick, 2015), ATOMS (Dowty, 2006) and publCIF (Westrip, 2010).