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. 2017 May 23;73(Pt 6):867–870. doi: 10.1107/S2056989017007186
Bruker D8 Quest diffractometer 3697 independent reflections
Radiation source: microfocus sealed tube (Incoatec ImS) 3509 reflections with I > 2σ(I)
Multi-layer mirror monochromator Rint = 0.024
Detector resolution: 10.24 pixels mm-1 θmax = 26.4°, θmin = 2.6°
φ and ω scans h = −10→10
Absorption correction: multi-scan (SADABS; Bruker, 2014) k = −19→19
Tmin = 0.718, Tmax = 0.746 l = −17→17
48705 measured reflections