Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C23H18FNO4 |
| M r | 391.38 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 100 |
| a, b, c (Å) | 8.4849 (11), 15.407 (3), 14.157 (2) |
| β (°) | 102.598 (16) |
| V (Å3) | 1806.1 (5) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.11 |
| Crystal size (mm) | 0.28 × 0.20 × 0.18 |
| Data collection | |
| Diffractometer | Bruker D8 Quest |
| Absorption correction | Multi-scan (SADABS; Bruker, 2014 ▸) |
| T min, T max | 0.718, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 48705, 3697, 3509 |
| R int | 0.024 |
| (sin θ/λ)max (Å−1) | 0.625 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.032, 0.081, 1.05 |
| No. of reflections | 3697 |
| No. of parameters | 264 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.38, −0.21 |