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. 2017 May 26;73(Pt 6):876–879. doi: 10.1107/S2056989017007381
Cl1A—C8A 1.764 (2) C7A—H7A 0.9300
Cl1B—C8B 1.761 (2) C9A—H9A 0.9300
N1A—C3A 1.337 (2) C11A—H11A 0.9300
N1A—N2A 1.376 (2) C12A—H12A 0.9300
N2A—C1A 1.352 (2) C13A—H13A 0.9300
N3A—C4A 1.408 (2) C14A—H14A 0.9300
N3A—C3A 1.395 (2) C15A—H15A 0.9300
N4A—C5A 1.422 (3) C1B—C2B 1.381 (3)
C1A—C10A 1.486 (2) C1B—C10B 1.482 (2)
C1A—C2A 1.383 (3) C2B—C3B 1.417 (2)
C2A—C3A 1.412 (2) N2B—H2NB 0.87 (2)
N2A—H2NA 0.87 (2) N3B—H3NB 0.830 (19)
N3A—H3NA 0.817 (18) C4B—C9B 1.395 (3)
C4A—C9A 1.395 (2) C4B—C5B 1.424 (3)
N4A—H4NB 0.91 (2) N4B—H4ND 0.89 (2)
N4A—H4NA 0.88 (2) N4B—H4NC 0.89 (2)
C4A—C5A 1.419 (3) C5B—C6B 1.394 (3)
C5A—C6A 1.395 (3) C6B—C7B 1.389 (3)
C6A—C7A 1.391 (3) C7B—C8B 1.386 (3)
C7A—C8A 1.391 (3) C8B—C9B 1.388 (3)
C8A—C9A 1.389 (3) C10B—C11B 1.396 (3)
C10A—C15A 1.398 (3) C10B—C15B 1.395 (3)
C10A—C11A 1.394 (3) C11B—C12B 1.390 (3)
C11A—C12A 1.391 (3) C12B—C13B 1.388 (3)
C12A—C13A 1.388 (3) C13B—C14B 1.376 (3)
C13A—C14A 1.378 (3) C14B—C15B 1.397 (3)
C14A—C15A 1.396 (3) C2B—H2B 0.9300
N1B—N2B 1.375 (2) C6B—H6B 0.9300
N1B—C3B 1.333 (2) C7B—H7B 0.9300
C2A—H2A 0.9300 C9B—H9B 0.9300
N2B—C1B 1.355 (2) C11B—H11B 0.9300
N3B—C4B 1.406 (2) C12B—H12B 0.9300
N3B—C3B 1.394 (2) C13B—H13B 0.9300
N4B—C5B 1.425 (3) C14B—H14B 0.9300
C6A—H6A 0.9300 C15B—H15B 0.9300
N2A—N1A—C3A 104.40 (14) C10A—C15A—H15A 120.00
N1A—N2A—C1A 112.47 (15) C14A—C15A—H15A 120.00
C3A—N3A—C4A 126.32 (15) N2B—C1B—C2B 105.97 (15)
N2A—C1A—C2A 106.40 (15) N2B—C1B—C10B 123.35 (17)
N2A—C1A—C10A 122.97 (16) C2B—C1B—C10B 130.61 (16)
C2A—C1A—C10A 130.62 (16) C1B—C2B—C3B 105.88 (15)
C1A—C2A—C3A 105.54 (16) N1B—N2B—H2NB 117.3 (14)
N1A—N2A—H2NA 116.4 (13) C1B—N2B—H2NB 129.7 (14)
C1A—N2A—H2NA 131.1 (13) N1B—C3B—N3B 118.36 (15)
N1A—C3A—N3A 118.34 (15) C3B—N3B—C4B 126.95 (16)
C3A—N3A—H3NA 114.6 (13) C3B—N3B—H3NB 115.5 (13)
C4A—N3A—H3NA 115.0 (13) C4B—N3B—H3NB 115.1 (13)
N1A—C3A—C2A 111.19 (16) N1B—C3B—C2B 110.95 (16)
N3A—C3A—C2A 130.28 (17) N3B—C3B—C2B 130.52 (17)
H4NB—N4A—H4NA 110.1 (18) H4ND—N4B—H4NC 107.7 (19)
C5A—C4A—C9A 119.52 (16) C5B—C4B—C9B 119.60 (17)
C5A—N4A—H4NA 109.1 (14) C5B—N4B—H4NC 109.7 (13)
N3A—C4A—C5A 117.59 (15) N3B—C4B—C5B 117.48 (16)
N3A—C4A—C9A 122.89 (16) N3B—C4B—C9B 122.91 (17)
C5A—N4A—H4NB 109.5 (13) C5B—N4B—H4ND 109.8 (13)
N4A—C5A—C4A 119.00 (16) N4B—C5B—C4B 119.34 (16)
N4A—C5A—C6A 121.84 (17) N4B—C5B—C6B 122.04 (17)
C4A—C5A—C6A 119.08 (16) C4B—C5B—C6B 118.54 (17)
C5A—C6A—C7A 121.47 (18) C5B—C6B—C7B 121.84 (18)
C6A—C7A—C8A 118.55 (18) C6B—C7B—C8B 118.58 (19)
C7A—C8A—C9A 121.61 (17) C7B—C8B—C9B 121.69 (18)
Cl1A—C8A—C7A 119.48 (15) Cl1B—C8B—C7B 119.31 (16)
Cl1A—C8A—C9A 118.89 (15) Cl1B—C8B—C9B 118.99 (15)
C4A—C9A—C8A 119.77 (17) C4B—C9B—C8B 119.74 (17)
C1A—C10A—C11A 119.28 (17) C1B—C10B—C11B 119.94 (17)
C1A—C10A—C15A 122.31 (16) C1B—C10B—C15B 122.19 (16)
C11A—C10A—C15A 118.41 (16) C11B—C10B—C15B 117.84 (16)
C10A—C11A—C12A 120.49 (19) C10B—C11B—C12B 120.82 (19)
C11A—C12A—C13A 120.58 (19) C11B—C12B—C13B 120.38 (18)
C12A—C13A—C14A 119.55 (19) C12B—C13B—C14B 119.74 (18)
C13A—C14A—C15A 120.23 (19) C13B—C14B—C15B 119.86 (19)
C10A—C15A—C14A 120.73 (18) C10B—C15B—C14B 121.34 (17)
N2B—N1B—C3B 104.53 (14) C1B—C2B—H2B 127.00
C3A—C2A—H2A 127.00 C3B—C2B—H2B 127.00
C1A—C2A—H2A 127.00 C5B—C6B—H6B 119.00
N1B—N2B—C1B 112.66 (16) C7B—C6B—H6B 119.00
C3B—N3B—C4B 126.95 (16) C6B—C7B—H7B 121.00
C5A—C6A—H6A 119.00 C8B—C7B—H7B 121.00
C7A—C6A—H6A 119.00 C4B—C9B—H9B 120.00
C8A—C7A—H7A 121.00 C8B—C9B—H9B 120.00
C6A—C7A—H7A 121.00 C10B—C11B—H11B 120.00
C8A—C9A—H9A 120.00 C12B—C11B—H11B 120.00
C4A—C9A—H9A 120.00 C11B—C12B—H12B 120.00
C10A—C11A—H11A 120.00 C13B—C12B—H12B 120.00
C12A—C11A—H11A 120.00 C12B—C13B—H13B 120.00
C11A—C12A—H12A 120.00 C14B—C13B—H13B 120.00
C13A—C12A—H12A 120.00 C13B—C14B—H14B 120.00
C14A—C13A—H13A 120.00 C15B—C14B—H14B 120.00
C12A—C13A—H13A 120.00 C10B—C15B—H15B 119.00
C13A—C14A—H14A 120.00 C14B—C15B—H15B 119.00
C15A—C14A—H14A 120.00
C3A—N1A—N2A—C1A −0.5 (2) C3B—N1B—N2B—C1B −1.2 (2)
N2A—N1A—C3A—N3A −175.01 (16) N2B—N1B—C3B—N3B −174.38 (17)
N2A—N1A—C3A—C2A 0.5 (2) N2B—N1B—C3B—C2B 1.2 (2)
N1A—N2A—C1A—C2A 0.2 (2) N1B—N2B—C1B—C2B 0.7 (2)
N1A—N2A—C1A—C10A −178.67 (16) N1B—N2B—C1B—C10B 178.09 (17)
C4A—N3A—C3A—N1A −149.84 (18) C4B—N3B—C3B—N1B −156.03 (18)
C4A—N3A—C3A—C2A 35.7 (3) C4B—N3B—C3B—C2B 29.4 (3)
C3A—N3A—C4A—C5A −162.61 (18) C3B—N3B—C4B—C5B −164.28 (18)
C3A—N3A—C4A—C9A 18.2 (3) C3B—N3B—C4B—C9B 16.9 (3)
N2A—C1A—C2A—C3A 0.1 (2) N2B—C1B—C2B—C3B 0.1 (2)
C10A—C1A—C2A—C3A 178.87 (19) C10B—C1B—C2B—C3B −177.05 (19)
N2A—C1A—C10A—C11A −163.29 (18) N2B—C1B—C10B—C11B 169.08 (19)
N2A—C1A—C10A—C15A 17.6 (3) N2B—C1B—C10B—C15B −12.8 (3)
C2A—C1A—C10A—C11A 18.1 (3) C2B—C1B—C10B—C11B −14.3 (3)
C2A—C1A—C10A—C15A −161.0 (2) C2B—C1B—C10B—C15B 163.8 (2)
C1A—C2A—C3A—N1A −0.4 (2) C1B—C2B—C3B—N1B −0.8 (2)
C1A—C2A—C3A—N3A 174.43 (19) C1B—C2B—C3B—N3B 174.08 (19)
N3A—C4A—C5A—N4A −2.4 (3) N3B—C4B—C5B—N4B −2.3 (3)
N3A—C4A—C5A—C6A −179.06 (17) N3B—C4B—C5B—C6B −179.09 (17)
C9A—C4A—C5A—N4A 176.89 (17) C9B—C4B—C5B—N4B 176.51 (17)
C9A—C4A—C5A—C6A 0.2 (3) C9B—C4B—C5B—C6B −0.3 (3)
N3A—C4A—C9A—C8A 179.43 (17) N3B—C4B—C9B—C8B 178.98 (18)
C5A—C4A—C9A—C8A 0.2 (3) C5B—C4B—C9B—C8B 0.2 (3)
N4A—C5A—C6A—C7A −177.36 (18) N4B—C5B—C6B—C7B −177.05 (19)
C4A—C5A—C6A—C7A −0.7 (3) C4B—C5B—C6B—C7B −0.4 (3)
C5A—C6A—C7A—C8A 0.9 (3) C5B—C6B—C7B—C8B 1.0 (3)
C6A—C7A—C8A—Cl1A 177.79 (15) C6B—C7B—C8B—Cl1B 177.56 (16)
C6A—C7A—C8A—C9A −0.4 (3) C6B—C7B—C8B—C9B −1.1 (3)
Cl1A—C8A—C9A—C4A −178.35 (14) Cl1B—C8B—C9B—C4B −178.18 (15)
C7A—C8A—C9A—C4A −0.1 (3) C7B—C8B—C9B—C4B 0.5 (3)
C1A—C10A—C11A—C12A −179.78 (18) C1B—C10B—C11B—C12B 177.10 (18)
C15A—C10A—C11A—C12A −0.6 (3) C15B—C10B—C11B—C12B −1.1 (3)
C1A—C10A—C15A—C14A 179.10 (17) C1B—C10B—C15B—C14B −177.09 (18)
C11A—C10A—C15A—C14A −0.1 (3) C11B—C10B—C15B—C14B 1.0 (3)
C10A—C11A—C12A—C13A 0.8 (3) C10B—C11B—C12B—C13B 0.2 (3)
C11A—C12A—C13A—C14A −0.3 (3) C11B—C12B—C13B—C14B 0.8 (3)
C12A—C13A—C14A—C15A −0.4 (3) C12B—C13B—C14B—C15B −0.8 (3)
C13A—C14A—C15A—C10A 0.5 (3) C13B—C14B—C15B—C10B −0.1 (3)