| Agilent Xcalibur Sapphire3 diffractometer | 4795 independent reflections |
| Radiation source: Enhance (Mo) X-ray Source | 3132 reflections with I > 2σ(I) |
| Detector resolution: 16.1827 pixels mm-1 | Rint = 0.027 |
| ω–scan | θmax = 25.0°, θmin = 2.5° |
| Absorption correction: multi-scan (CrysAlis RED; Agilent, 2012). | h = −11→11 |
| Tmin = 0.649, Tmax = 1.000 | k = −24→24 |
| 15157 measured reflections | l = −16→15 |
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