| Stoe IPDS 2T diffractometer | 1653 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.056 |
| Detector resolution: 6.67 pixels mm-1 | θmax = 25.0°, θmin = 2.1° |
| area detector scans | h = −6→6 |
| 3731 measured reflections | k = −11→11 |
| 1774 independent reflections | l = −12→12 |
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