| Agilent Xcalibur, Atlas, Nova diffractometer | 2053 independent reflections |
| Radiation source: fine-focus sealed tube | 2012 reflections with I > 2σ(I) |
| Detector resolution: 10.3543 pixels mm-1 | Rint = 0.026 |
| ω scans | θmax = 75.0°, θmin = 5.1° |
| Absorption correction: multi-scan (CrysAlis PRO, Agilent, 2003) | h = −9→9 |
| Tmin = 0.919, Tmax = 1.000 | k = −10→10 |
| 28193 measured reflections | l = −9→11 |
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