| Stoe IPDS 2T diffractometer | 1596 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.062 |
| Detector resolution: 6.67 pixels mm-1 | θmax = 25.0°, θmin = 2.1° |
| area detector scans | h = −8→8 |
| 4194 measured reflections | k = −9→9 |
| 1904 independent reflections | l = −11→11 |
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