| Refinement on F2 | 0 restraints |
| Least-squares matrix: full | w = 1/[σ2(Fo2) + (0.0121P)2 + 3.2851P] where P = (Fo2 + 2Fc2)/3 |
| R[F2 > 2σ(F2)] = 0.020 | (Δ/σ)max = 0.001 |
| wR(F2) = 0.047 | Δρmax = 1.47 e Å−3 |
| S = 1.19 | Δρmin = −0.92 e Å−3 |
| 2137 reflections | Extinction correction: SHELXL2014 (Sheldrick, 2015b), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4 |
| 99 parameters | Extinction coefficient: 0.00102 (10) |