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. 2017 May 26;73(Pt 6):890–892. doi: 10.1107/S205698901700740X

Table 1. Experimental details.

Crystal data
Chemical formula Ag1.655Co1.64Fe1.36(PO4)3
M r 2544.10
Crystal system, space group Monoclinic, C2/c
Temperature (K) 296
a, b, c (Å) 11.8680 (3), 12.5514 (3), 6.4386 (2)
β (°) 114.012 (1)
V3) 876.09 (4)
Z 1
Radiation type Mo Kα
μ (mm−1) 9.51
Crystal size (mm) 0.31 × 0.26 × 0.22
 
Data collection
Diffractometer Bruker X8 APEX
Absorption correction Multi-scan (SADABS; Krause et al., 2015)
T min, T max 0.066, 0.124
No. of measured, independent and observed [I > 2σ(I)] reflections 13097, 2137, 2079
R int 0.030
(sin θ/λ)max−1) 0.833
 
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S 0.020, 0.047, 1.19
No. of reflections 2137
No. of parameters 99
Δρmax, Δρmin (e Å−3) 1.47, −0.92

Computer programs: APEX2 aand SAINT (Bruker, 2009), SHELXT2014 (Sheldrick, 2015a ), SHELXL2014 (Sheldrick, 2015b ), ORTEP-3 for Windows (Farrugia, 2012), DIAMOND (Brandenburg, 2006) and publCIF (Westrip, 2010).