Table 1. Experimental details.
| Crystal data | |
| Chemical formula | CaNi2Fe(PO4)3 |
| M r | 498.26 |
| Crystal system, space group | Orthorhombic, I m m a |
| Temperature (K) | 296 |
| a, b, c (Å) | 10.3126 (3), 13.1138 (3), 6.4405 (2) |
| V (Å3) | 871.00 (4) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 7.14 |
| Crystal size (mm) | 0.30 × 0.27 × 0.21 |
| Data collection | |
| Diffractometer | Bruker X8 APEX |
| Absorption correction | Multi-scan (SADABS; Krause et al., 2015 ▸) |
| T min, T max | 0.596, 0.748 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 8446, 1171, 1153 |
| R int | 0.020 |
| (sin θ/λ)max (Å−1) | 0.840 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.017, 0.044, 1.17 |
| No. of reflections | 1171 |
| No. of parameters | 54 |
| Δρmax, Δρmin (e Å−3) | 0.76, −0.63 |