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. 2017 May 26;73(Pt 6):896–900. doi: 10.1107/S2056989017007460
O1—C7 1.2187 (17) C7—C8 1.474 (2)
O2—C1 1.364 (2) C8—C9 1.3267 (19)
O2—C13 1.419 (2) C8—H8A 0.9300
C1—C2 1.387 (2) C9—C10 1.4616 (19)
C1—C6 1.396 (2) C9—H9A 0.9300
C2—C3 1.378 (3) C10—C12 1.3897 (19)
C2—H2A 0.9300 C10—C11 1.4002 (19)
C3—C4 1.370 (3) C11—C12i 1.3760 (19)
C3—H3A 0.9300 C11—H11A 0.9300
C4—C5 1.375 (2) C12—C11i 1.3761 (19)
C4—H4A 0.9300 C12—H12A 0.9300
C5—C6 1.387 (2) C13—H13A 0.9600
C5—H5A 0.9300 C13—H13B 0.9600
C6—C7 1.4932 (19) C13—H13C 0.9600
C1—O2—C13 118.66 (14) C9—C8—C7 120.50 (13)
O2—C1—C2 124.22 (16) C9—C8—H8A 119.8
O2—C1—C6 115.79 (13) C7—C8—H8A 119.8
C2—C1—C6 119.87 (16) C8—C9—C10 127.89 (13)
C3—C2—C1 119.34 (18) C8—C9—H9A 116.1
C3—C2—H2A 120.3 C10—C9—H9A 116.1
C1—C2—H2A 120.3 C12—C10—C11 118.03 (13)
C4—C3—C2 121.72 (17) C12—C10—C9 122.99 (12)
C4—C3—H3A 119.1 C11—C10—C9 118.97 (12)
C2—C3—H3A 119.1 C12i—C11—C10 121.57 (12)
C3—C4—C5 118.73 (19) C12i—C11—H11A 119.2
C3—C4—H4A 120.6 C10—C11—H11A 119.2
C5—C4—H4A 120.6 C11i—C12—C10 120.40 (12)
C4—C5—C6 121.43 (18) C11i—C12—H12A 119.8
C4—C5—H5A 119.3 C10—C12—H12A 119.8
C6—C5—H5A 119.3 O2—C13—H13A 109.5
C5—C6—C1 118.81 (14) O2—C13—H13B 109.5
C5—C6—C7 117.92 (14) H13A—C13—H13B 109.5
C1—C6—C7 123.27 (14) O2—C13—H13C 109.5
O1—C7—C8 121.49 (13) H13A—C13—H13C 109.5
O1—C7—C6 119.30 (13) H13B—C13—H13C 109.5
C8—C7—C6 119.12 (12)
C13—O2—C1—C2 −4.7 (2) C5—C6—C7—O1 −36.6 (2)
C13—O2—C1—C6 179.21 (14) C1—C6—C7—O1 143.60 (15)
O2—C1—C2—C3 −174.24 (17) C5—C6—C7—C8 140.06 (15)
C6—C1—C2—C3 1.7 (3) C1—C6—C7—C8 −39.8 (2)
C1—C2—C3—C4 0.8 (3) O1—C7—C8—C9 −13.5 (2)
C2—C3—C4—C5 −1.5 (3) C6—C7—C8—C9 169.90 (14)
C3—C4—C5—C6 −0.4 (3) C7—C8—C9—C10 178.03 (14)
C4—C5—C6—C1 2.8 (2) C8—C9—C10—C12 −13.8 (2)
C4—C5—C6—C7 −177.02 (15) C8—C9—C10—C11 167.44 (15)
O2—C1—C6—C5 172.83 (13) C12—C10—C11—C12i 0.1 (2)
C2—C1—C6—C5 −3.4 (2) C9—C10—C11—C12i 178.90 (13)
O2—C1—C6—C7 −7.4 (2) C11—C10—C12—C11i −0.1 (2)
C2—C1—C6—C7 176.38 (14) C9—C10—C12—C11i −178.84 (13)