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. 2017 May 26;73(Pt 6):896–900. doi: 10.1107/S2056989017007460
Bruker APEXII DUO CCD area-detector diffractometer 2183 independent reflections
Radiation source: fine-focus sealed tube 1705 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.024
φ and ω scans θmax = 26.8°, θmin = 1.7°
Absorption correction: multi-scan (SADABS; Bruker, 2012) h = −8→8
Tmin = 0.883, Tmax = 0.985 k = −24→31
8322 measured reflections l = −7→7