Bruker APEXII DUO CCD area-detector diffractometer | 3165 independent reflections |
Radiation source: fine-focus sealed tube | 2328 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.030 |
φ and ω scans | θmax = 29.0°, θmin = 1.9° |
Absorption correction: multi-scan (SADABS; Bruker, 2012) | h = −9→8 |
Tmin = 0.890, Tmax = 0.985 | k = −28→26 |
12532 measured reflections | l = −11→11 |