Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C26H38N5P |
| M r | 451.58 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 150 |
| a, b, c (Å) | 10.0148 (12), 17.343 (2), 15.6270 (19) |
| β (°) | 105.948 (2) |
| V (Å3) | 2609.7 (5) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.13 |
| Crystal size (mm) | 0.39 × 0.35 × 0.27 |
| Data collection | |
| Diffractometer | Siemens/Bruker APEXII |
| Absorption correction | Multi-scan (SADABS; Bruker, 2008 ▸) |
| T min, T max | 0.718, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 29851, 5708, 4350 |
| R int | 0.047 |
| (sin θ/λ)max (Å−1) | 0.639 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.046, 0.123, 1.02 |
| No. of reflections | 5708 |
| No. of parameters | 291 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.36, −0.39 |