Table 4.
Solvents | Low | Middle | High |
---|---|---|---|
Ethyl acetate | 66% | 70% | 65% |
Methanol-tetrahydrofuran (1:1) | 70% | 67% | 65% |
Methanol –trichloromethane (1:1) |
70% |
72% |
71% |
Methanol |
A great deal of impure peaks |
||
Acetone- ethyl acetate (2:1) | 80% | 82% | 78% |
Acetone -ethyl acetate (1:1) | 81% | 80% | 83% |
Acetone -ethyl acetate (1:2) | 82% | 81% | 83% |