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. 2016 Dec 29;82(3):1538–1544. doi: 10.1021/acs.joc.6b02737

Figure 3.

Figure 3

EPR (v = 9.6505 GHz) spectrum of 0.1 mM nitroxide 1 in chloroform. (Top panel) Complete spectrum; (bottom panel) expansion plot near the center peak showing 13C satellite peaks. Simulation: g = 2.0062, A(14N) = 34.2 MHz (n = 1), A(1H) = 1.10 MHz (n = 2), A(15N) = 48.1 MHz (n = 1), A(13C) = 25.3 MHz (n = 4), A(13C) = 15.5 MHz (n = 2), Lorentzian/Gaussian = 0.4, LW = 0.020 mT (all nuclei are at natural abundance).