Fig. 5. RP-HPLC analysis of products formed from 13S-HPOTE by Fg-cat.
Products were chromatographed using a Waters Symmetry C18 column (0.46 × 25 cm), a solvent of CH3CN/water/glacial acetic acid (60:40:0.01 by volume) at a flow rate of 1 mL/min, with the UV profiles depicted at 235 nm (red) and 280 nm (black). The main peaks were further purified by SP-HPLC and the structures established by LC-MS and 1H-NMR (Supplement Fig. S3, Tables S3–S6).