Table 1.
HPLC conditions for LC-MS/MS.
Compound | Time (min) | Flow velocity (μL/min) | Mobile phase B (%) | Mobile phase A (%) |
---|---|---|---|---|
Cefazolin | 0 | 600 | 1 | 99 |
impurity G | 6.0 | 600 | 30 | 70 |
impurity H | 8.0 | 600 | 80 | 20 |
impurity I | 10.0 | 600 | 80 | 20 |
impurity J | 10.1 | 600 | 1 | 99 |
impurity K | 15.0 | 600 | 1 | 99 |
impurity M | ||||
impurity N | ||||
impurity A | 0 | 600 | 5 | 95 |
impurity F | 10.0 | 600 | 5 | 95 |