Table 2.
Compound | R2 | R3 | Yield [%][a] |
---|---|---|---|
18p | NHAc | OH | 76 |
18d | OH | F | 50 |
18q | F | F | 55 |
18r | OH | Cl | 41 |
18s | F | Cl | 41 |
18t | OH | 3‐NO2, 4‐OH | 25[b] |
18u | OH | 3‐OH, 4‐NO2 | 58 |
18v | OH | 4‐COOH | 60 |
18w | OH | 4‐NH2 | 64 |
18x | OH | 4‐EtOCOCH2O | 54 |
viniferifuran 2 | OH | 4‐OH | 64 |
[a] Isolated yield.
[b] Purified by HPLC.