Table 1. Results of the O-ATRP of MMA Using PCs 1 through 4a.
run no. | PC | conv (%) | Mw (kDa) | Mn (kDa) | dispersity (Đ) | I* (%) |
---|---|---|---|---|---|---|
1 | 1 | 95.6 | 10.6 | 7.2 | 1.48 | 137 |
2 | 2 | 55.3 | 9.5 | 6.5 | 1.45 | 85.5 |
3 | 3 | 78.8 | 10.8 | 8.8 | 1.22 | 92.6 |
4 | 4 | 80.2 | 11.9 | 10.8 | 1.11 | 77.3 |
[MMA]:[DBMM]:[PC] = [1000]:[10]:[1]; 9.35 μmol PC, 1.00 mL dimethylacetamide, and irradiated with a 54 W 365 nm light source for 8 h.