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. Author manuscript; available in PMC: 2018 Apr 26.
Published in final edited form as: ACS Appl Mater Interfaces. 2017 Apr 13;9(16):14478–14489. doi: 10.1021/acsami.6b15006

Figure 5.

Figure 5

Effects of reactant concentrations and reaction temperature on the physical properties of Zol-Ca complexes synthesized in RM. (A) Representative TEM micrographs of Zol-Ca complexes synthesized in RM with a fixed concentration ratio of CaCl2/Zol at 7.5/1, but different concentrations of CaCl2 and Zol (i.e. 0.375 M/0.05 M (A-1) or 0.6 M/0.08 M (A-2)); or with a fixed CaCl2 concentration of 0.15 M, but different concentrations of Zol (i.e. 0.05M (A-3) or 0.08M (A-4)). (B) Representative TEM micrographs of Zol-Ca complexes synthesized in RM with a reaction temperature of ~30 °C or ~10 °C (bars = 100 nm).