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. 2017 Jul 28;1508:16–23. doi: 10.1016/j.chroma.2017.05.050

Table 2.

Molar mass moments of linear PNIPAM prepared using Fe ATRP over nine repeat measurements using SEC with methanol as eluent. S.D. = standard deviation; C.V. = coefficient of variation.

Repeat MNa Mwa Mza Ð k/dl g−1 α
1.1 18.74 28.75 37.56 1.53 0.00408 0.66
1.2 18.53 27.76 37.05 1.50 0.00378 0.67
1.3 18.07 27.61 37.32 1.53 0.00398 0.67
2.1 17.85 27.93 37.81 1.56 0.00412 0.66
2.2 18.81 28.26 37.76 1.50 0.00398 0.67
2.3 18.29 28.5 37.75 1.56 0.00384 0.66
3.1 18.41 27.31 36.74 1.48 0.003999 0.67
3.2 18.55 28.12 37.57 1.52 0.00391 0.66
3.3 18.55 27.53 37.24 1.48 0.00377 0.66
Mean 18.42 27.97 37.42 1.48 0.00394 0.664
S.D. 0.31 0.47 0.36 0.02 0.00012 0.005
C.V 0.017 0.017 0.010 0.014 0.031 0.008
a

Polymer molar mass in kg mol−1.