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. 2017 May 22;56(25):7161–7165. doi: 10.1002/anie.201703369

Table 4.

Aniline deprotection in flow.[a] Inline graphic

graphic file with name ANIE-56-7161-g009.jpg

[a] Reaction conditions: 0.5 mmol product (6) in 5.0 mL HCl (32 wt %)/1,4‐dioxane (1:1), added to the PFA reactor by syringe pump (for 7 af R1=Me, for 7 g,h R2=Me). Aniline obtained after extraction procedure (no chromatography).