Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C8H5FN2O2 |
| M r | 180.14 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 200 |
| a, b, c (Å) | 7.3036 (10), 7.2045 (10), 14.009 (2) |
| β (°) | 94.736 (4) |
| V (Å3) | 734.61 (18) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.14 |
| Crystal size (mm) | 0.34 × 0.32 × 0.06 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD area detector |
| Absorption correction | Multi-scan (SADABS; Krause et al., 2015 ▸) |
| T min, T max | 0.663, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 8386, 2142, 1687 |
| R int | 0.021 |
| (sin θ/λ)max (Å−1) | 0.705 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.040, 0.108, 1.05 |
| No. of reflections | 2142 |
| No. of parameters | 126 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.30, −0.21 |
Computer programs: APEX2 and SAINT (Bruker, 2014 ▸), SHELXT2014/4 (Sheldrick, 2015a ▸), SHELXL2016/6 (Sheldrick, 2015b ▸), WinGX (Farrugia, 2012 ▸), DIAMOND (Brandenburg, 2006 ▸), GOLD (Chen et al., 2015 ▸), MOPAC (Stewart, 2016 ▸), CRYSTAL EXPLORER (Wolff, et al., 2012 ▸), publCIF (Westrip, 2010 ▸) and enCIFer (Allen et al., 2004 ▸).