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. 2017 Jun 16;73(Pt 7):1041–1043. doi: 10.1107/S2056989017008738
Oxford Diffraction Xcalibur Eos diffractometer 5040 independent reflections
Radiation source: fine-focus sealed X-ray tube 4503 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.032
Detector resolution: 16.1419 pixels mm-1 θmax = 31.1°, θmin = 2.5°
ω–scan h = −12→11
Absorption correction: multi-scan (CrysAlis PRO; Rigaku Oxford Diffraction, 2015) k = −14→14
Tmin = 0.952, Tmax = 1.000 l = −15→15
45592 measured reflections