Oxford Diffraction Xcalibur Eos diffractometer | 5040 independent reflections |
Radiation source: fine-focus sealed X-ray tube | 4503 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.032 |
Detector resolution: 16.1419 pixels mm-1 | θmax = 31.1°, θmin = 2.5° |
ω–scan | h = −12→11 |
Absorption correction: multi-scan (CrysAlis PRO; Rigaku Oxford Diffraction, 2015) | k = −14→14 |
Tmin = 0.952, Tmax = 1.000 | l = −15→15 |
45592 measured reflections |