Table 4. Experimental details.
| Crystal data | |
| Chemical formula | C26H25N |
| M r | 351.47 |
| Crystal system, space group | Triclinic, P
|
| Temperature (K) | 100 |
| a, b, c (Å) | 11.0758 (8), 12.4989 (11), 14.2425 (13) |
| α, β, γ (°) | 98.088 (3), 96.537 (3), 102.151 (3) |
| V (Å3) | 1887.2 (3) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.07 |
| Crystal size (mm) | 0.73 × 0.12 × 0.10 |
| Data collection | |
| Diffractometer | Bruker APEX II CCD |
| Absorption correction | – |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 37669, 9087, 6437 |
| R int | 0.052 |
| (sin θ/λ)max (Å−1) | 0.661 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.049, 0.131, 1.04 |
| No. of reflections | 9087 |
| No. of parameters | 500 |
| No. of restraints | 7 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.28, −0.36 |