Table 1.
Unit Cell Parameters
| entry | sample | [DIPA]c | a (Å) | b (Å) | c (Å) | β (deg) |
|---|---|---|---|---|---|---|
| 1a | 1·PhNO2 | – | 34.37 ± 0.77 | 14.99 ± 0.10 | 30.55 ± 0.41 | 100.93 ± 0.83 |
| 2a | 1·DIPA | neat | 36.39 ± 0.21 | 14.70 ± 0.03 | 30.53 ± 0.12 | 101.90 ± 0.32 |
| 3b | 1·PhNO2 | – | 34.219(2) | 15.002(1) | 30.331(2) | 100.567(5) |
| 4 | 1·DIPA | 48 M | 36.966(7) | 14.695(8) | 30.906(4) | 102.626(4) |
| 5 | 1·DIPA | 23 M | 37.085(3) | 14.666(1) | 30.858(2) | 102.546(5) |
| 6 | 1·DIPA | 12 M | 37.024(5) | 14.718(2) | 30.883(9) | 102.706(13) |
| 7 | 1·DIPA | 5.3 M | 37.018(11) | 14.668(2) | 30.809(5) | 102.471(6) |
| 8 | 1·DIPA | 1.3 M | 37.174(19) | 14.764(2) | 30.539(6) | 102.885(21) |
| 9 | 1·DIPA | 0.1 M | 37.266(9) | 14.801(1) | 30.471(6) | 103.229(14) |
| 10 | 1·DIPA | 0.05 M | 37.167(11) | 14.799(2) | 30.481(5) | 102.987(17) |