Table 1. Experiments Used To Train the Kinetic Model^a.

entry	Ni(cod)2 content (mol %)	temperature (°C)	concentration (M)	maximum conversionb (%)	time (h)
1	10.0	40	0.66	92	8
2	10.0	33	0.66	70	6
3	10.0	50	0.66	91	4
4	0.5	65	1.16	77	8
5	0.1	80	1.16	13	1

^aAll reactions were performed on a 0.50–1.00 mmol scale, with respect to amide 1, using 1.2 equiv (−)-menthol (2) and a 1:1 ratio of Ni(cod)₂:SIPr in toluene.¹⁰

^bConversion was determined by SFC analysis, using biphenyl as an internal standard.