. Author manuscript; available in PMC: 2017 Nov 4.

Published in final edited form as: Org Lett. 2016 Oct 18;18(21):5449–5451. doi: 10.1021/acs.orglett.6b02722

Table 2.

Aminoacetoxylation of Aliphatic Amines


entry	amine substrate	product	yeild (%)^b
1	1a	2a	69
2	1b	2b	75
3	1c	2c	83

Amine substrate (0.5 mmol) treated with PdCl₂(PhCN)₂ (5 mol %), Cu(NO₃)₂•3H₂O (5 mol %) in AcOH/Ac₂O (6:1, 10.5 mL) under an O₂ atmosphere (1 atm) at 23 °C for 16 h.

Yield of isolated product.