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. Author manuscript; available in PMC: 2018 Jun 1.
Published in final edited form as: Phytochem Lett. 2017 Apr 15;20:54–60. doi: 10.1016/j.phytol.2017.03.012

Table 2.

1H (700 MHz) and 13C (175 MHz) NMR spectroscopic dataa for 3,5,3-trihydroxy-7,4-dimethoxy-6,8-C-dimethyl-flavone (2).

Position δC δH, m (J in Hz) HMBCb
 2 145.8
 3 136.2
 4 175.9
 5 156.0
 6 113.4
 7 163.0c
 8 109.4
 9 152.4
 10 105.8
 1′ 124.6
 2′ 113.7 7.82, d (2.1) C-2, C-6′
 3′ 145.8
 4′ 148.4
 5′ 110.7 7.00, d (9.1) C-1′, C-3′
 6′ 121.1 7.87, dd (9.1, 2.1) C-2, C-2′
 6-CH3 8.4 2.23, s C-5, C-6, C-7
 8-CH3 8.7 2.41, s C-7, C-8, C-9
 7-OCH3 60.8 3.80, s C-7
 4′-OCH3 56.2 4.00, s C-4′
 3-OH 6.64 C-3, C-4
 3′-OH 5.71 C-2′, C-3′
 5-OH 11.80 C-5, C-10
a1

H and 13C chemical shifts with reference to CDCl3 (δH = 7.26 ppm) and CDCl3 (δC = 77.16 ppm), respectively.

b

HMBC correlations are from the proton stated to the indicated carbon.

c

obtained from HMBC