Table 2.
List of sIgA HR O-glycopeptides
RT (min) | Base Peak (Da) | Z | Error (ppm) | Formula | Hex | HexNAc | Neu5Ac | Relative intensity (%) |
---|---|---|---|---|---|---|---|---|
22.35 | 1441.7946 | 5 | −3.5 | C294 H459 N59 O143 S3 | 6 | 6 | 3 | 0.07 |
22.12 | 1383.5586 | 5 | −15.9 | C283 H442 N58 O135 S3 | 6 | 6 | 2 | 0.07 |
21.93 | 1325.1411 | 5 | −15.4 | C272 H425 N57 O127 S3 | 6 | 6 | 1 | 0.04 |
23.12 | 1467.5875 | 5 | −14.1 | C299 H466 N60 O146 S3 | 6 | 5 | 4 | 0.15 |
22.55 | 1409.3685 | 5 | −14.6 | C288 H449 N59 O138 S3 | 6 | 5 | 3 | 0.45 |
22.28 | 1351.1494 | 5 | −15.3 | C277 H432 N58 O130 S3 | 6 | 5 | 2 | 0.57 |
22.04 | 1292.9313 | 5 | −15.2 | C266 H415 N57 O122 S3 | 6 | 5 | 1 | 0.32 |
21.76 | 1234.7120 | 5 | −16.1 | C255 H398 N56 O114 S3 | 6 | 5 | 0 | 0.08 |
23.40 | 1435.1755 | 5 | −15.4 | C293 H456 N60 O141 S3 | 6 | 4 | 4 | 0.38 |
22.83 | 1376.9572 | 5 | −15.5 | C282 H439 N59 O133 S3 | 6 | 4 | 3 | 1.64 |
22.49 | 1318.7403 | 5 | −14.6 | C271 H422 N58 O125 S3 | 6 | 4 | 2 | 1.35 |
22.25 | 1260.1283 | 5 | −9.6 | C260 H405 N57 O117 S3 | 6 | 4 | 1 | 0.31 |
21.95 | 1502.3845 | 4 | −10.2 | C249 H388 N56 O109 S3 | 6 | 4 | 0 | 0.14 |
23.59 | 1344.5323 | 5 | −26.5 | C276 H429 N59 O128 S3 | 6 | 3 | 3 | 0.94 |
23.20 | 1286.3315 | 5 | −13.5 | C265 H412 N58 O120 S3 | 6 | 3 | 2 | 1.15 |
22.81 | 1227.9189 | 5 | −8.9 | C254 H395 N57 O112 S3 | 6 | 3 | 1 | 0.70 |
22.43 | 1169.7008 | 5 | −8.5 | C243 H378 N56 O104 S3 | 6 | 3 | 0 | 0.34 |
24.71 | 1485.1758 | 5 | −24.0 | C302 H470 N60 O149 S3 | 5 | 5 | 5 | 0.59 |
23.72 | 1427.1532 | 5 | −27.4 | C291 H453 N59 O141 S3 | 5 | 5 | 4 | 1.87 |
23.19 | 1368.7517 | 5 | −15.7 | C280 H436 N58 O133 S3 | 5 | 5 | 3 | 2.39 |
22.78 | 1310.5358 | 5 | −14.0 | C269 H419 N57 O125 S3 | 5 | 5 | 2 | 2.21 |
22.39 | 1252.3178 | 5 | −13.8 | C258 H402 N56 O117 S3 | 5 | 5 | 1 | 1.56 |
22.10 | 1193.9069 | 5 | −7.6 | C247 H385 N55 O109 S3 | 5 | 5 | 0 | 0.57 |
24.56 | 1452.7646 | 5 | −24.9 | C296 H460 N60 O144 S3 | 5 | 4 | 5 | 0.10 |
24.18 | 1394.5549 | 5 | −19.2 | C285 H443 N59 O136 S3 | 5 | 4 | 4 | 6.72 |
23.69 | 1336.3333 | 5 | −21.9 | C274 H426 N58 O128 S3 | 5 | 4 | 3 | 9.20 |
23.13 | 1278.1190 | 5 | −19.2 | C263 H409 N57 O120 S3 | 5 | 4 | 2 | 7.93 |
22.65 | 1219.7091 | 5 | −12.6 | C252 H392 N56 O112 S3 | 5 | 4 | 1 | 5.30 |
22.29 | 1161.4932 | 5 | −10.5 | C241 H375 N55 O104 S3 | 5 | 4 | 0 | 1.85 |
24.41 | 1303.9263 | 5 | −19.8 | C268 H416 N58 O123 S3 | 5 | 3 | 3 | 3.78 |
23.93 | 1245.5141 | 5 | −15.2 | C257 H399 N57 O115 S3 | 5 | 3 | 2 | 4.08 |
23.27 | 1187.3040 | 5 | −8.4 | C246 H382 N56 O107 S3 | 5 | 3 | 1 | 2.48 |
22.76 | 1129.0857 | 5 | −8.1 | C235 H365 N55 O99 S3 | 5 | 3 | 0 | 0.68 |
24.79 | 1213.1057 | 5 | −13.8 | C251 H389 N57 O110 S3 | 5 | 2 | 2 | 0.33 |
24.10 | 1154.8932 | 5 | −8.8 | C240 H372 N56 O102 S3 | 5 | 2 | 1 | 0.37 |
25.42 | 1412.1573 | 5 | −19.6 | C288 H447 N59 O139 S3 | 4 | 4 | 5 | 0.27 |
25.14 | 1353.9268 | 5 | −28.9 | C277 H430 N58 O131 S3 | 4 | 4 | 4 | 6.64 |
24.74 | 1295.7254 | 5 | −16.5 | C266 H413 N57 O123 S3 | 4 | 4 | 3 | 6.67 |
24.14 | 1237.5065 | 5 | −17.1 | C255 H396 N56 O115 S3 | 4 | 4 | 2 | 5.48 |
23.46 | 1179.0949 | 5 | −11.6 | C244 H379 N55 O107 S3 | 4 | 4 | 1 | 3.20 |
22.87 | 1120.8728 | 5 | −15.0 | C233 H362 N54 O99 S3 | 4 | 4 | 0 | 0.96 |
25.65 | 1321.5394 | 5 | −12.0 | C271 H420 N58 O126 S3 | 4 | 3 | 4 | 0.31 |
25.54 | 1263.3206 | 5 | −12.4 | C260 H403 N57 O118 S3 | 4 | 3 | 3 | 4.12 |
25.13 | 1204.8921 | 5 | −20.7 | C249 H386 N56 O110 S3 | 4 | 3 | 2 | 3.67 |
24.34 | 1146.6773 | 5 | −18.1 | C238 H369 N55 O102 S3 | 4 | 3 | 1 | 1.63 |
23.56 | 1088.4603 | 5 | −17.2 | C227 H352 N54 O94 S3 | 4 | 3 | 0 | 0.50 |
26.05 | 977.2487 | 6 | −8.2 | C243 H376 N56 O105 S3 | 4 | 2 | 2 | 0.16 |
24.69 | 928.7259 | 6 | −16.0 | C232 H359 N55 O97 S3 | 4 | 2 | 1 | 0.06 |
25.75 | 1222.5168 | 5 | −2.9 | C252 H390 N56 O113 S3 | 3 | 3 | 3 | 2.60 |
25.16 | 1164.2785 | 5 | −19.5 | C241 H373 N55 O105 S3 | 3 | 3 | 2 | 1.62 |
24.18 | 1106.2704 | 5 | −10.7 | C230 H356 N54 O97 S3 | 3 | 3 | 1 | 0.24 |
26.16 | 1131.8795 | 5 | −9.9 | C235 H363 N55 O100 S3 | 3 | 2 | 2 | 1.09 |
28.19 | 1199.5245 | 4 | −8.6 | C202 H310 N52 O77 S3 | 1 | 1 | 1 | 0.06 |
28.80 | 1035.4722 | 4 | −5.6 | C177 H270 N50 O59 S3 | 0 | 0 | 0 | 0.02 |