Table 2.

Results obtained with the system combining the two‐step synthesis with purification.

Entry	Sample intake method	Yield[a] [%]	Purity[b] [%]	Productivity[c] [g h−1 L−1]
1	two‐phase[d]	57	>99.9	1.44
2	one‐phase[e]	59	>99.9	2.27

[a] Yield of isolated product for the two synthetic steps followed by quasi‐continuous purification. [b] Determined by GCMS. [c] Mass of the pure product divided by the time of the process and the volume of the column. [d] Schematically shown in Figure 3 A. [e] Schematically shown in Figure 3 B.