Table 1.
Analyte | Concentration range (μg mL−1) | Calibration curve | LOD (μg mL−1) | LOQ (μg mL−1) | Spiked level (μg mL−1) | Precision, RSD% | Relative recovery, % (RSD, %) (n = 5) | |
---|---|---|---|---|---|---|---|---|
Intraday (n = 5) | Interday (n = 5) | |||||||
Oleanolic acid | 1–160 | y = 2611x − 909.59 | 0.36 | 1.2 | 12 | 1.95 | 2.55 | 109.0 (0.38) |
24 | 97.4 (3.32) | |||||||
36 | 108.2 (3.18) | |||||||
Ursolic acid | 2–320 | y = 1950x + 6240.8 | 0.18 | 0.6 | 60 | 1.48 | 1.18 | 101.6 (4.10) |
120 | 99.2 (2.53) | |||||||
180 | 111.4 (7.14) |