TABLE III.
Table representing the experimental conditions (factors) and thiol content (response) obtained from disulfide tests for each experiment using response-surface design
| Run | Factor A: EDC | Factor B: Amine | Response: Thiol Content |
|---|---|---|---|
| (moles) | (moles) | (in % of Derivatization of HA) | |
| 16 | 0.5 | 0.5 | 6.80 |
| 3 | 10 | 0.5 | 15.74 |
| 14 | 0.5 | 10 | 7.61 |
| 12 | 10 | 10 | 27.5 |
| 10 | 5.25 | 10 | 22.52 |
| 4 | 10 | 5.25 | 26.33 |
| 5 | 5.25 | 2.88 | 23.95 |
| 11 | 0.5 | 5.25 | 5.52 |
| 15 | 2.88 | 7.63 | 25.89 |
| 7 | 7.63 | 7.63 | 37.12 |
| 9 | 5.25 | 0.5 | 21.47 |
| 8 | 0.5 | 0.5 | 6.82 |
| 13 | 10 | 0.5 | 24.87 |
| 2 | 0.5 | 10 | 7.65 |
| 1 | 10 | 10 | 34.50 |
| 6 | 10 | 5.25 | 36.34 |